Introduction to X-Ray Powder Diffractometry.pdf

Introduction to X-Ray Powder Diffractometry PDF

Ron Jenkins

When bombarded with X-rays, solid materials produce distinct scattering patterns similar to fingerprints. X-ray powder diffraction is a technique used to fingerprint solid samples, which are then identified and cataloged for future use-much the way the FBI keeps fingerprints on file. The current database of some 70,000 material prints has been put to a broad range of uses, from the analysis of moon rocks to testing drugs for purity. Introduction to X-ray Powder Diffractometry fully updates the achievements in the field over the past fifteen years and provides a much-needed explanation of the state-of-the-art techniques involved in characterizing materials. It covers the latest instruments and methods, with an emphasis on the fundamentals of the diffractometer, its components, alignment, calibration, and automation. The first three chapters outline diffraction theory in clear language, accessible to both students and professionals in chemistry, physics, geology, and materials science. The books middle chapters describe the instrumentation and procedures used in X-ray diffraction, including X-ray sources, X-ray detection, and production of monochromatic radiation. The chapter devoted to instrument design and calibration is followed by an examination of specimen preparation methods, data collection, and reduction. The final two chapters provide in-depth discussions of qualitative and quantitative analysis. While the material is presented in an orderly progression, beginning with basic concepts and moving on to more complex material, each chapter stands on its own and can be studied independently or used as a professional reference. More than 230 illustrations and tables demonstrate techniques and clarify complex material. Self-contained, timely, and user-friendly, Introduction to X-ray Powder Diffractometry is an enormously useful text and professional reference for analytical chemists, physicists, geologists and materials scientists, and upper-level undergraduate and graduate students in materials science and analytical chemistry. X-ray powder diffraction-a technique that has matured significantly in recent years-is used to identify solid samples and determine their composition by analyzing the so-called "e

Introduction to X-ray Powder Diffractometry, a collaboration between two internationally known and respected experts in the field, provides invaluable guidance to anyone using X-ray powder diffractometers and diffractometry in materials science, ceramics, the pharmaceutical industry, and elsewhere.

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Introduction to X-Ray Powder Diffractometry.pdf


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Sofia Voigt

(prepared by James R. Connolly, for EPS400-001, Introduction to X-Ray Powder Diffraction, Spring 2007 (Material in this document is borrowed from many sources; all original material is ©2007 by James R. Connolly) (Revision date: 10-Feb-07) Page 2 of 18 scatter x … Introduction to X-Ray Powder Diffractometry | …

Matteo Müller

Book Review Introduction to X-Ray Powder Diffractometry, Ron Jenkins and Robert L. Snyder, John Wiley and Sons, New York 1996, ISBN 0 471 51339 3, 403+XXIII pp. Chapter 1 Diffraction and the X-Ray Powder Diffractometer

Noel Schulze

plication areas for X-ray powder diffractometry far ... The intro- duction of the rotating anode X-ray tube offered some improvement by allowing maximum tube.

Jason Lehmann

An Introduction to Quantum Microwaves for Communication and Sensing · Making the TEM more Relevant for Catalysis Research. Jennifer McConnell. Identification of different crystalline phases and the determination of their relative concentrations in mixtures based on the diffraction pattern analysis recorded ...

Jessica Kohmann

Quantitative Determination of Airborne Respirable … 30.04.2009 · The application of X-ray powder diffractometry makes it possible to determine the exposure to SiC dust for compliance work. Here, we report on a method for quantitative determination of non-fibrous SiC dust by X-ray powder diffractometry. MATERIALS AND METHODS Material samples